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61.
Renjith Devasia CP Reghunadhan Nair P Sivadasan KN Ninan 《Polymer International》2005,54(8):1110-1118
Polyacrylonitrile terpolymers of various compositions consisting of acrylonitrile (AN), itaconic acid (IA) and methyl acrylate (MA) were synthesized by solution polymerization in dimethylsulfoxide. Increase in concentration of either IA or MA retarded the overall polymerization rate and the polymer molecular weight. The system consisting of AN + MA and varying IA concentration was more prone to retardation in comparison with the system composed of AN + IA with variable MA concentration. The retardation factors were quantified. Minor quantities of MA boost the reactivity of IA in the terpolymer system. The terpolymer was richer in MA vis‐à‐vis the feed. The thermal characteristics of the terpolymer were examined as a function of its composition. In contrast to the copolymer of AN and IA requiring 1–1.5 mol% IA, the terpolymer required an IA content of approximately 2.5 mol% for optimum thermal stability. The polymer with 90 mol% AN, 2.5 mol% IA and 7.5 mol% MA exhibited reasonably good char‐forming characteristics and thermal stability. The overall crystallinity and crystallite size of the polymers were found to decrease on incorporation of the comonomers. The ‘aromatization index’ of the copolymer increased with the temperature of pyrolysis through re‐organization of the tetrahydropyridine ladder structure. Copyright © 2005 Society of Chemical Industry 相似文献
62.
Polyelectrolite hydrogels are crosslinked polymers which display high sorption capacity in water and water solutions. They are widely used in the marked of personal hygiene products, as well as in other biomedical and industrial applications. In the most industrial application they are not biodegradable and prepared starting from acrylamide.In this work, the chemical-physical analysis of a novel class of natural polymers-based microporous superabsorbent hydrogels has been presented. The main focus is the definition of the relationship between material's chemical-physical structure and its equilibrium sorption properties.The effect of the variation of the degree of crosslinking, the polyelectrolyte nature of the backbone and the hydrogel microporosity on its swelling properties has been analysed, and a good agreement with the theoretical statements has been displayed.The effect of the ionic strength and the pH of the external solution in contact with the hydrogel on its equilibrium sorption properties has also been assessed, and an high sensitivity to these variations was detected for all the tested chemical compositions and physical structures.This work have to be considered part of the efforts towards the reduction of the environmental impact of the large scale consumption industrial polymer based products. 相似文献
63.
在薄板坯连铸连轧流程上,经过对Ti微合金化技术研究,有效解决了Ti微合金化强度性能波动大的问题,开发出屈服强度450~700MPa高强钢。对试制钢组织性能和工业应用分析研究,表明该产品通板性能良好,通板强度差30MPa左右;成形性能良好,d=0时冷弯测试全部合格;同时还具有良好焊接性能,焊接后,强度波动较小,均在母材部位断开;试制钢显微组织为珠光体和铁素体,晶粒均匀细小,平均尺寸为4~8/μm;实物质量满足集装箱和汽车制造行业要求,具有广阔市场前景。 相似文献
64.
Wang Xuegang Yan Fengjie Yan Qian Li Xingeng 《Frontiers of Materials Science in China》2007,1(2):225-227
An iron-based amorphous foil (FeNiCrSiB) was used as an interlayer for the amorphous diffusion bonding of low carbon steel
pipes under argon flux. The microstructure and mechanical properties of the joint were analyzed using an electron probe micro-analyzer
(EPMA), tensile test, bending test and impact test. The results show that the joint microstructure resembles that of the base
metal and no precipitates form at the joint. Melting point depressants (B, Si) diffuse far away from the joint and the base
metal element is homogenous across the joint. The joint impact toughness is greater than the base metal toughness and the
mechanical properties of the joint are similar around the pipe. 相似文献
65.
Atmospheric corrosion of reference metals in Antarctic sites 总被引:1,自引:0,他引:1
Manuel Morcillo Beln Chico Daniel de la Fuente Elisabete Almeida Günter Joseph Susana Rivero Blanca Rosales 《Cold Regions Science and Technology》2004,40(3):165-178
This paper presents the results obtained at three Antarctic test sites participating in the “Ibero-American Map of Atmospheric Corrosiveness” (MICAT), a project on atmospheric corrosion carried out during the period 1988–1994 at some 70 sites distributed across 12 countries of the Latin-American region, Spain and Portugal. The three Antarctic sites are located near the coastline.The singular climatic characteristics of Antarctic regions are related with the purity of the air, the absence of rainfall and the formation of ice on the metallic surface during an important part of the exposure time. However, electrochemical activity is possible below ice layers. This situation affects the structure and morphology of corrosion product films and the resulting corrosion rates of metallic surfaces. 相似文献
66.
67.
在由低压直流电源供电的电路中,往往电路的某些部位需要使用高于电源所供的电压,将电源所供的低压转换为较高的电压,常用的方法有3种:自举升压、电感升压、逆变升压。结合实际应用电路对各种升压方法从器件选择、升压原理、升压结果等诸方面进行分析、探讨,解决了总体供电电压不变时,局部高压产生的关键性问题。它对电子电器电路的设计人员有一定的启发作用,对优化电路、遴选器件有较强的参考价值。 相似文献
68.
Iwao Shimizu Yuji Naito Iwao Yamaguchi Katsuyuki Kaiho Hitoshi Mizoguchi Satoru Yanabu 《Electrical Engineering in Japan》2008,164(1):52-61
Using conventional high‐temperature superconducting wire, a model superconducting fault current limiter (SFCL) is made and tested. Solenoid coil using Bi2223 silver sheath wire is so made that inductance is as small as possible and a vacuum interrupter is connected in series to it. A conventional reactor coil is connected in parallel. When the fault current flows in this equipment, superconducting wire is quenched and current is transferred into the parallel coil because of voltage drop of superconducting wire. This large current in parallel coil actuates magnetic repulsion mechanism of vacuum interrupter. Due to opening of vacuum interrupter, the current in superconducting wire is broken. By using this equipment, current flow time in superconducting wire can be easily minimized. On the other hand, the fault current is also easily limited by large reactance of parallel coil. © 2008 Wiley Periodicals, Inc. Electr Eng Jpn, 164(1): 52–61, 2008; Published online in Wiley InterScience ( www.interscience.wiley.com ). DOI 10.1002/eej.20315 相似文献
69.
70.
The present study is an investigation on the behaviors of concrete-filled thin-walled steel tubular members subjected to combined loading, such as compression and torsion, bending and torsion, compression, bending and torsion. ABAQUS software is used in this paper for the finite element analysis (FEA). A comparison of results calculated using this modeling shows generally good agreement with test results. The FEA modeling is then used to investigate the influence of important parameters that determine the ultimate strength of the composite members under combined loading, such as compression and torsion, bending and torsion, compression, bending and torsion. The parametric studies provide information for the development of formulae for calculating the ultimate strength of the composite members subjected to combined loading. 相似文献